Phosphorus oxide (P4O10) → 1-Decyl-2,3-difluorobenzene
反応式
[F:1][C:2]1[C:7]([F:8])=[CH:6][CH:5]=[CH:4][C:3]=1[CH:9](O)[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18].O=P12OP3(OP(OP(O3)(O1)=O)(=O)O2)=O>[Pd]>[F:1][C:2]1[C:7]([F:8])=[CH:6][CH:5]=[CH:4][C:3]=1[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18]参加物
4
実験手順
Quantities: compound from Example 21 (56.4 g, 0.21 mol), phosphorus pentoxide (74.5 g, 0.53 mol) and 5% palladium-on-charcoal (4.58). The experimental procedure was as described in Example 22.
出典と根拠
- ORDレコード
- ord-500d918177684402bdf015e9f0b33816
- 出典データセット
- uspto-grants-1997_11
- 特許番号
- US05683623
反応ノート
読み込み中…