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HRID 2297361作成日:2026年10月27日

tert-Butyl methacrylate → 3-[tris(trimethylsilyloxy)silyl]propyl methacrylate t-butyl methacrylate 5-oxo-4-oxatricyclo[4.2.1.03,7]nonan-2-yl Methacrylate

https://huagongshe.com/reaction/2297361

反応式

関与物質

役割名称HCID仕込み量
反応物tert-Butyl methacrylateHCID 11448—
反応物3-(Tris(trimethylsiloxy)silyl)propyl methacrylateHCID 123371—
反応物1,4,4-Trimethyl-4-silacyclohexyl methacrylateHCID 18381205—
生成物3-[tris(trimethylsilyloxy)silyl]propyl methacrylate t-butyl methacrylate 5-oxo-4-oxatricyclo[4.2.1.03,7]nonan-2-yl MethacrylateHCID 70157708—

反応手順

A copolymer was synthesized as in Polymer Synthesis Example 1 except that 3-[tris(trimethylsilyloxy)silyl]propyl methacrylate and t-butyl methacrylate were used instead of 1,4,4-trimethyl-4-silacyclohexyl methacrylate. The polymer was confirmed by the light scattering method to have a weight average molecular weight of 13,000 g/mol and by the GPC elution curve to have a dispersity (Mw/Mn) of 1.78. By 1H-NMR analysis, the copolymer was found to contain the components in a ratio of approximately 2:5:3.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US06492089B2
出典データセットuspto-grants-2002_12
ORD IDord-f11f81e9aa554f2595304d658ef37647
出典メモuspto-grants-2002_12