Benzyl Isothiocyanate → 4-benzyl-3-[(4-chlorobenzyl)thio]-5-(2-furyl)-4H-1,2,4-triazole

HRID 229766

反応式

HRID 229766 の反応式
[O:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[C:6]([NH:8][NH2:9])=O.[CH2:10]([N:17]=[C:18]=[S:19])[C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1.[Cl:20][C:21]1[CH:28]=[CH:27][C:24]([CH2:25]Br)=[CH:23][CH:22]=1>>[CH2:10]([N:17]1[C:6]([C:2]2[O:1][CH:5]=[CH:4][CH:3]=2)=[N:8][N:9]=[C:18]1[S:19][CH2:25][C:24]1[CH:27]=[CH:28][C:21]([Cl:20])=[CH:22][CH:23]=1)[C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1

参加物

4

反応物 3

HCID 2346Benzyl IsothiocyanateHCID 187312-Furancarboxylic acid, hydrazideHCID 693291-(Bromomethyl)-4-chlorobenzene

生成物 1

HCID 71818094-benzyl-3-[(4-chlorobenzyl)thio]-5-(2-furyl)-4H-1,2,4-triazole

実験手順

This compound was synthesized using the same methodology as described in Example 1 above, using 2-furancarboxylic acid hydrazide, benzyl isothiocyanate and 4-chlorobenzyl bromide as the starting materials. (M+H)+−382.

後処理

  1. customThis compound was synthesized

出典と根拠

ORDレコード
ord-efda426bc2cb4df8961b54a77e95ad08
出典データセット
uspto-grants-2009_07
特許番号
US07563905B2

関連ノート

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