Benzyl Isothiocyanate → 2-[4-benzyl-5-(4-chloro-benzylsulfanyl)-4H-1,2,4-triazol-3-yl]pyridine

HRID 229771

反応式

HRID 229771 の反応式
[N:1]1[CH:6]=[CH:5][CH:4]=[CH:3][C:2]=1[C:7]([NH:9][NH2:10])=O.[CH2:11]([N:18]=[C:19]=[S:20])[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1.[Cl:21][C:22]1[CH:29]=[CH:28][C:25]([CH2:26]Br)=[CH:24][CH:23]=1>>[CH2:11]([N:18]1[C:19]([S:20][CH2:26][C:25]2[CH:28]=[CH:29][C:22]([Cl:21])=[CH:23][CH:24]=2)=[N:10][N:9]=[C:7]1[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][N:1]=1)[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1

参加物

4

反応物 3

HCID 2346Benzyl IsothiocyanateHCID 693291-(Bromomethyl)-4-chlorobenzeneHCID 255881Picolinohydrazide

生成物 1

HCID 113268242-[4-benzyl-5-(4-chloro-benzylsulfanyl)-4H-1,2,4-triazol-3-yl]pyridine

実験手順

This compound was synthesized using the same methodology as described in Example 1 above, using 2-pyridinecarboxylic acid hydrazide, benzyl isothiocyanate and 4-chlorobenzyl bromide as the starting materials.

後処理

  1. customThis compound was synthesized

出典と根拠

ORDレコード
ord-01bae73466824536ac177382e56d03ea
出典データセット
uspto-grants-2009_07
特許番号
US07563905B2

関連ノート

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