Methanol → Propylene Glycol

HRID 229895

反応式

HRID 229895 の反応式
[CH3:1][O-:2].[Na+].[CH2:4]([OH:8])[CH:5]([OH:7])[CH3:6].[CH3:9][OH:10].CO>C1(=O)OC(C)CO1>[CH2:4]([OH:8])[CH:5]([OH:7])[CH3:6].[C:4](=[O:8])([O:10][CH3:9])[O:2][CH3:1]

参加物

6

実験手順

In a process as described in FIG. 1 7 t/h (tonnes per hour) propylene carbonate is fed into the upper part of a reactive distillation zone. Sodium methanolate in 0.5 t/h propylene glycol/methanol mixture as transesterification catalyst is also passed into the upper part of zone in an amount of 0.05 t/h. Twenty t/h methanol, fed into a lower part of the distillation zone, passes upward, and reacts with the propylene carbonate to form propylene glycol product and dimethyl carbonate. The propylene glycol is recovered in an amount of 5 t/h.

出典と根拠

ORDレコード
ord-92e778977c1649e1ab96e2996ca52116
出典データセット
uspto-grants-2009_07
特許番号
US07563919B2

関連ノート

読み込み中…