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Maleic Anhydride → Tert-butyl 5-norbornene-2-carboxylate alpha-[hydroxy(5-norbornen-2-yl)methyl]-gamma-butyrolactone maleic anhydride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Maleic Anhydride | HCID 7923 | — |
| 反応物 | 2,2'-Azobis(2,4-dimethylvaleronitrile) | HCID 91537 | — |
| 反応物 | Bicyclo[2.2.1]hept-5-ene-2-carboxylic acid, 1,1-dimethylethyl ester | HCID 15607334 | — |
| 反応物 | 3-[(Bicyclo[2.2.1]hept-5-en-2-yl)(hydroxy)methyl]oxolan-2-one | HCID 18345689 | — |
| 生成物 | Tert-butyl 5-norbornene-2-carboxylate alpha-[hydroxy(5-norbornen-2-yl)methyl]-gamma-butyrolactone maleic anhydride | HCID 86584390 | — |
反応手順
Polymerization reaction of tert-butyl 5-norbornene-2-carboxylate, Monomer 1, and maleic anhydride was effected using 2,2′-azobis(2,4-dimethylvaleronitrile) as the initiator, yielding an alternating copolymer of tert-butyl 5-norbornene-2-carboxylate/α-[hydroxy(5-norbornen-2-yl)methyl]-γ-butyrolactone/maleic anhydride (copolymerization ratio 4/1/5).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06500961B2 |
| 出典データセット | uspto-grants-2002_12 |
| ORD ID | ord-d61fc84b384e4c3fa7c9daff40847b54 |
| 出典メモ | uspto-grants-2002_12 |