HCID 13935155、化合物 → 1-Acridinol, 1,2,3,4-tetrahydro-9-amino-6-(trifluoromethyl)-
反応式
[NH2:1][C:2]1[C:3]2[C:8]([N:9]=[C:10]3[C:15]=1[C:14](=[O:16])[CH2:13][CH2:12][CH2:11]3)=[CH:7][C:6]([C:17]([F:20])([F:19])[F:18])=[CH:5][CH:4]=2.[H-].[Al+3].[Li+].[H-].[H-].[H-]>O1CCCC1>[NH2:1][C:2]1[C:3]2[C:8]([N:9]=[C:10]3[C:15]=1[CH:14]([OH:16])[CH2:13][CH2:12][CH2:11]3)=[CH:7][C:6]([C:17]([F:20])([F:18])[F:19])=[CH:5][CH:4]=2参加物
4
実験手順
9-Amino-3,4-dihydro-6-trifluoromethylacridin-1(2H)-one (2.4 g) was suspended in 60 ml of tetrahydrofuran. To this cooled solution was added 9 ml of 1 molar solution of lithium aluminum hydride in THF. This was stirred for 30 minutes.
出典と根拠
- ORDレコード
- ord-329b4c6c8bde480791b913b9ffc83c3c
- 出典データセット
- uspto-grants-1987_09
- 特許番号
- US04695573
反応ノート
読み込み中…