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HRID 231263作成日：2026年10月26日
Methyl Methanesulfonate → 2-[(2-Methoxy-3-octadecyloxypropyl)sulfonyl]ethyltrimethylammonium mesylate
https://huagongshe.com/reaction/231263
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Methyl Methanesulfonate | HCID 4156 | — |
| 反応物 | 2-[(2-Methoxy-3-octadecyloxypropyl)sulfonyl]ethyldimethylamine | HCID 14498265 | — |
| 溶媒 | Chloroform | HCID 6212 | — |
| 生成物 | 2-[(2-Methoxy-3-octadecyloxypropyl)sulfonyl]ethyltrimethylammonium mesylate | HCID 14498246 | 70.6% |
反応手順
In 10 ml of chloroform are dissolved 0.48 g of 2-[(2-methoxy-3-octadecyloxypropyl)sulfonyl]ethyldimethylamine and 1 g of methyl methanesulfonate and the solution is stirred at 70° C. for 5 hours. Then the reaction mixture is concentrated under reduced pressure and the residue is crystallized from chloroform and ether to give 417 mg of the captioned compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 特許番号 | US04845219 |
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| 出典データセット | uspto-grants-1989_07 |
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| ORD ID | ord-1c6f273932834c8c827785532613c3dc |
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| 出典メモ | uspto-grants-1989_07 |
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