Methyl iodide → 2-[(2-Methoxy-3-octadecyloxypropyl)sulfonyl]ethyltrimethylammonium iodide

HRID 231264ノート

反応式

HRID 231264 の反応式
[CH3:1][O:2][CH:3]([CH2:13][O:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH3:32])[CH2:4][S:5]([CH2:8][CH2:9][N:10]([CH3:12])[CH3:11])(=[O:7])=[O:6].[CH3:33][I:34]>CCOCC>[I-:34].[CH3:1][O:2][CH:3]([CH2:13][O:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH3:32])[CH2:4][S:5]([CH2:8][CH2:9][N+:10]([CH3:33])([CH3:12])[CH3:11])(=[O:6])=[O:7]

参加物

4

反応物 2

HCID 6328Methyl iodideHCID 144982652-[(2-Methoxy-3-octadecyloxypropyl)sulfonyl]ethyldimethylamine

生成物 1

HCID 144982482-[(2-Methoxy-3-octadecyloxypropyl)sulfonyl]ethyltrimethylammonium iodide

試薬・触媒・溶媒 1

HCID 3283Diethyl Ether溶媒

実験手順

In 5 ml of ether is dissolved 0.24 g of 2-[(2-methoxy-3-octadecyloxypropyl)sulfonyl]ethyldimethylamine to which is added 1 ml of methyl iodide. The solution is then stirred at room temperature for 2 days. The reaction liquid is concentrated under reduced pressure and the residue is treated with methanol to give 275 mg of the captioned compound as powder.

後処理

  1. customThe reaction liquid
  2. concentrationis concentrated under reduced pressure
  3. additionthe residue is treated with methanol

出典と根拠

ORDレコード
ord-c41443b41d0f4024954fde2ad444d8d1
出典データセット
uspto-grants-1989_07
特許番号
US04845219

反応ノート

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