1H-1,2,4-Triazole → HCID 10679259、化合物
反応式
Cl[C:2]1[N:7]=[C:6]([O:8][CH3:9])[CH:5]=[C:4]([CH3:10])[N:3]=1.[NH:11]1[CH:15]=[N:14][CH:13]=[N:12]1>O1CCCC1>[CH3:9][O:8][C:6]1[CH:5]=[C:4]([CH3:10])[N:3]=[C:2]([N:11]2[CH:15]=[N:14][CH:13]=[N:12]2)[N:7]=1参加物
4
実験手順
In anhydrous tetrahydrofuran, 159 mg of 2-chloro-4-methoxy-6-methylpyrimidine was substituted with 69 mg of 1,2,4-triazole. The reaction mixture was treated according to the procedure as in Example 5 to yield 92 mg of 4-methoxy-6-methyl-2-(1,2,4-triazol-1-yl)-pyrimidine, recrystallized from n-hexane, having a melting point of 142.5°-143° C.
後処理
- additionThe reaction mixture was treated
出典と根拠
- ORDレコード
- ord-ea28cb82fec64b66bd289f086b02e378
- 出典データセット
- uspto-grants-1989_07
- 特許番号
- US04849424
反応ノート
読み込み中…