HCID 14555602、化合物 → HCID 14555603、化合物
反応式
[N+:1]([C:4]1[CH:20]=[CH:19][C:7]([O:8][CH:9]([CH3:18])[CH2:10][CH2:11][N:12]2[CH2:17][CH2:16][O:15][CH2:14][CH2:13]2)=[CH:6][CH:5]=1)([O-])=O>[OH-].[OH-].[Pd+2].C(O)C>[CH3:18][CH:9]([O:8][C:7]1[CH:6]=[CH:5][C:4]([NH2:1])=[CH:20][CH:19]=1)[CH2:10][CH2:11][N:12]1[CH2:13][CH2:14][O:15][CH2:16][CH2:17]1参加物
4
実験手順
To 50 mL ethanol is added 28 g (0.1 mol) of 4-[3-(4-nitrophenoxy)butyl]morpholine and 0.5 g of Pd(OH)2. The mixture is hydrogenated at 30 psi. Monitor the reaction by thin-layer chromatography. Upon completion remove the catalyst by suction filtration through celite. Remove the solvent in vacuo to obtain the title compound.
後処理
- customMonitor the reaction by thin-layer chromatography
- customUpon completion remove the catalyst
- filtrationby suction filtration through celite
- customRemove the solvent in vacuo
出典と根拠
- ORDレコード
- ord-af78acccf56d4bb3a6a4bf583c6b820c
- 出典データセット
- uspto-grants-1989_07
- 特許番号
- US04851526
反応ノート
読み込み中…