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HRID 234071作成日:2026年10月26日

1,3-Bis(4-methylphenyl)prop-2-en-1-one → 1-Methyl-4-[3-(4-methylphenyl)propyl]benzene

https://huagongshe.com/reaction/234071

反応式

関与物質

役割名称HCID仕込み量
反応物1,3-Bis(4-methylphenyl)prop-2-en-1-oneHCID 256552—
触媒PalladiumHCID 23938—
溶媒Acetic AcidHCID 176—
生成物1-Methyl-4-[3-(4-methylphenyl)propyl]benzeneHCID 57172699.4%

反応手順

To a suspension of 2.14 g of 4,4'-dimethylchalcone in 40 ml of acetic acid was added 0.2 g of 5% palladium on carbon. The reaction vessel was purged with hydrogen gas, and the mixture was vigorously stirred at room temperature for 8.5 hours. The reaction mixture was filtered through Celite, and the filtrate was concentrated to give 2.02 g of the title compound.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US05594081
出典データセットuspto-grants-1997_01
ORD IDord-9c59153766d74092b67b123096222700
出典メモuspto-grants-1997_01