化工社化工社 化学情報印刷レポート · 研究参考用
Nitric Acid → 4-Tert-butyl-1-methyl-2-nitrobenzene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Nitric Acid | HCID 944 | — |
| 反応物 | Sulfuric Acid | HCID 1118 | — |
| 反応物 | 4-tert-Butyltoluene | HCID 7390 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | 4-Tert-butyl-1-methyl-2-nitrobenzene | HCID 10954415 | — |
反応手順
Nitration was performed as described in General Method 12 using tert-butyl-4-methylbenzene (25 g), concentrated H2SO4 (92 g), 70% HNO3 (82 g), and H2O (25 g). The crude product was purified via distillation under vacuum.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06852711B2 |
| 出典データセット | uspto-grants-2005_02 |
| ORD ID | ord-28047e1787ec4cb588412d11eb80d13c |
| 出典メモ | uspto-grants-2005_02 |