Sodium → HCID 13469244、化合物
反応式
[C:1]([N:5]1[C:10](=[O:11])[C:9]([Cl:12])=[C:8]([SH:13])[CH:7]=[N:6]1)([CH3:4])([CH3:3])[CH3:2].[Na].[C:15]([C:19]1[CH:27]=[CH:26][C:22]([CH:23](Cl)[CH3:24])=[CH:21][CH:20]=1)([CH3:18])([CH3:17])[CH3:16]>CN(C)C=O>[C:1]([N:5]1[C:10](=[O:11])[C:9]([Cl:12])=[C:8]([S:13][CH:23]([CH3:24])[C:22]2[CH:26]=[CH:27][C:19]([C:15]([CH3:18])([CH3:17])[CH3:16])=[CH:20][CH:21]=2)[CH:7]=[N:6]1)([CH3:4])([CH3:2])[CH3:3]参加物
5
実験手順
By conducting a procedure similar to that in Synthesis Example 3 except using 1.5 g of 2-tert.-butyl-4-chloro-5-mercapto-3(2H)-pyridazinone, 10 ml of N,N-dimethylformamide, 1.0 g of anhydrous sodium carbonte and 1.4 g of 4-tert.-butyl-α-methylbenzyl chloride, there were obtained white needle-like crystals having the following physical properties (yield: 72.7%):