Methanol → HCID 54335577、化合物
反応式
[CH2:1]([S:7][CH:8]=[CH:9][CH2:10]Cl)[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6].C(N(C(C)C)CC)(C)C.[CH3:21][OH:22]>CCCCCC>[CH3:21][O:22][CH2:10][CH:9]=[CH:8][S:7][CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH3:6]参加物
5
実験手順
3-Hexylthio-2-propenyl chloride is added to a solution of diisopropyl ethyl amine (3.68 g, 28.5 mmol) in 20 ml of methanol. The mixture is stirred overnight at RT. It is then diluted with hexane, washed with water and with brine and is stripped. The crude product is purified by prep. TLC to give 3-methoxy-1-hexylthio-1-propene.
後処理
- washwashed with water and with brine
- customThe crude product is purified by prep
出典と根拠
- ORDレコード
- ord-3f5b6b6e640848808e565dc80061b09b
- 出典データセット
- uspto-grants-1989_10
- 特許番号
- US04877899
反応ノート
読み込み中…