Hydrogen Bromide → 2,6-Diphenylpyridine hydrobromide

HRID 235609ノート

反応式

HRID 235609 の反応式
[BrH:1].[C:2]1([C:8]2[CH:13]=[CH:12][CH:11]=[C:10]([C:14]3[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=3)[N:9]=2)[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1>C1(C)C=CC=CC=1>[BrH:1].[C:14]1([C:10]2[CH:11]=[CH:12][CH:13]=[C:8]([C:2]3[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=3)[N:9]=2)[CH:15]=[CH:16][CH:17]=[CH:18][CH:19]=1

参加物

4

反応物 2

HCID 260Hydrogen Bromide2 回HCID 729202,6-Diphenylpyridine

生成物 1

HCID 202183212,6-Diphenylpyridine hydrobromide

試薬・触媒・溶媒 1

HCID 1140Toluene溶媒

実験手順

Hydrogen bromide gas is introduced into a solution of 30 g (0.130 mole) of 2,6-diphenylpyridine in 150 ml of toluene. The solid which forms is isolated by vacuum filtration. The filtrate is retreated with hydrogen bromide until no more solid is formed. The solid is then dried in vacuo. The product has a melting point of 161° C.-162° C.

後処理

  1. customThe solid which forms is isolated by vacuum filtration
  2. customis formed
  3. customThe solid is then dried in vacuo

出典と根拠

ORDレコード
ord-60faa63473cd46718136fe30ba636c9d
出典データセット
uspto-grants-1987_02
特許番号
US04640831

反応ノート

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