9,10-Dihydro-9,10-dioxo-1-anthracenesulfonic acid → Silver 9,10-anthraquinone-1-sulfonate

HRID 2356181

反応式

HRID 2356181 の反応式
[C:1]1([S:17]([O-:20])(=[O:19])=[O:18])[C:14]2[C:13](=[O:15])[C:12]3[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=3)[C:6](=[O:16])[C:5]=2[CH:4]=[CH:3][CH:2]=1.[Na+].C1(S(O)(=O)=O)C2C(=O)C3C(=CC=CC=3)C(=O)C=2C=CC=1.[Ag:42]=O>O>[C:1]1([S:17]([O-:20])(=[O:18])=[O:19])[C:14]2[C:13](=[O:15])[C:12]3[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=3)[C:6](=[O:16])[C:5]=2[CH:4]=[CH:3][CH:2]=1.[Ag+:42]

参加物

5

反応物 3

HCID 67139,10-Dihydro-9,10-dioxo-1-anthracenesulfonic acidHCID 92152Silver(II) oxideHCID 517266Sodium anthraquinone-1-sulfonate

生成物 1

HCID 86625862Silver 9,10-anthraquinone-1-sulfonate

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

Five parts of sodium 9,10-anthraquinone-1-sulfonate was dissolved in 400.0 parts of ion-exchanged water at 45° C. The obtained solution was, passed through a column packed with 6.9 parts of an ion-exchanged resin (DUOLITE C20) to obtain a solution containing 9,10-anthraquinone-1-sulfonic acid. To the obtained solution, 2.0 parts' of silver oxide was added and the resultant mixture was stirred over night. The mixture was filtrated to obtain 3.9 parts of silver 9,10-anthraquinone-1-sulfonate.

後処理

  1. customto obtain a solution
  2. filtrationThe mixture was filtrated

出典と根拠

ORDレコード
ord-d6eb375e76004d959da9c09b1d49e6d2
出典データセット
uspto-grants-2010_07
特許番号
US07759045B2

関連ノート

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