1,4-Dioxane → HCID 16045868、化合物
反応式
[NH2:1][C:2]1[CH:9]=[CH:8][C:7]([Cl:10])=[CH:6][C:3]=1[CH:4]=O.[CH3:11][O:12][C:13]1[CH:18]=[CH:17][CH:16]=[C:15]([O:19][CH3:20])[C:14]=1[CH2:21][CH2:22][C:23]#[N:24].O1CCOCC1>C(O)(C)(C)C>[Cl:10][C:7]1[CH:6]=[C:3]2[C:2](=[CH:9][CH:8]=1)[N:1]=[C:23]([NH2:24])[C:22]([CH2:21][C:14]1[C:15]([O:19][CH3:20])=[CH:16][CH:17]=[CH:18][C:13]=1[O:12][CH3:11])=[CH:4]2参加物
5
実験手順
The title compound was synthesized according to EXAMPLE 11 from 2-amino-5-chlorobenzaldehyde and 3-(2,6-dimethoxyphenyl)propionitrile. Instead of dioxane, tert-butanol was used from [sic; as]1 the solvent. 1TN: “aus” (from) appears to be a typo for “als” (as).
出典と根拠
- ORDレコード
- ord-e32dd35d1f9b47779c71041fe6378791
- 出典データセット
- uspto-grants-2014_04
- 特許番号
- US08686002B2
反応ノート
読み込み中…