Trimethylsilanol → Hexamethyldisiloxane
反応式
[CH3:1][Si:2]([CH3:5])([CH3:4])[OH:3]>C(OCC)C>[CH3:1][Si:2]([O:3][Si:2]([CH3:5])([CH3:4])[CH3:1])([CH3:5])[CH3:4]参加物
3
試薬・触媒・溶媒 1
実験手順
This reaction proceeds slowly without diethylether but reacts faster at reflux temperatures. Trimethylsilanol is condensed during the HMDS distillation step to give HMDSO, which reacts as shown above.
後処理
- customreacts faster
- temperatureat reflux temperatures
- customcondensed
- distillationduring the HMDS distillation step
出典と根拠
- ORDレコード
- ord-5481fd3911d649d58cd82ef099a34174
- 出典データセット
- uspto-grants-1987_02
- 特許番号
- US04644076
反応ノート
読み込み中…