HCID 25193405、化合物 → 934162-32-0
反応式
[NH2:1][C:2]1[C:10]([N+:11]([O-])=O)=[CH:9][C:8]([F:14])=[CH:7][C:3]=1[C:4]([NH2:6])=[O:5]>C1COCC1.C(O)C.[Ni]>[NH2:1][C:2]1[C:10]([NH2:11])=[CH:9][C:8]([F:14])=[CH:7][C:3]=1[C:4]([NH2:6])=[O:5]参加物
5
実験手順
To a solution of EXAMPLE 45C (11.2 g) in a mixture of THF (50 mL) and ethanol (50 mL) was added Raney nickel (50% in water, 11.0 g). The mixture was stirred under hydrogen (60 psi) for 5 hours. Solid material was filtered off and the filtrate was concentrated.
後処理
- filtrationSolid material was filtered off
- concentrationthe filtrate was concentrated
出典と根拠
- ORDレコード
- ord-61ea365c9aeb475584ace8a60f91860c
- 出典データセット
- uspto-grants-2014_04
- 特許番号
- US08697736B2
反応ノート
読み込み中…