Maleic Anhydride → Dibutyltin maleate

HRID 2380027ノート

反応式

HRID 2380027 の反応式
[C:1]1(=[O:7])[O:6][C:4](=[O:5])[CH:3]=[CH:2]1.[CH2:8]([Sn:12](=[O:17])[CH2:13][CH2:14][CH2:15][CH3:16])[CH2:9][CH2:10][CH3:11]>>[C:1]([O-:6])(=[O:7])/[CH:2]=[CH:3]\[C:4]([O-:17])=[O:5].[CH2:8]([Sn+2:12][CH2:13][CH2:14][CH2:15][CH3:16])[CH2:9][CH2:10][CH3:11]

参加物

3

反応物 2

HCID 7923Maleic AnhydrideHCID 61221Dibutyltin oxide

生成物 1

HCID 9906251Dibutyltin maleate

実験手順

A mixture of 2.28 kg of maleic anhydride and 5.97 kg of dibutyltin oxide is continuously added to a screw drier whose heat exchange areas consist of two heating and one cooling zone. Behind each heating zone, a suction device is present for removing any water of reaction which may be formed. The reaction mixture passes through both heating zones at an average residence time of 7.5 minutes, the temperature of the first heating zone being 68° C. and that of the second one being 63° C., and is then cooled to 25°-30° C. At the exit of the screw drier, dibutyltin maleate (compound 3), is obtained as a white free-flowing powder.

後処理

  1. additionis continuously added to a screw drier whose
  2. temperatureheat exchange areas
  3. customfor removing
  4. customany water of reaction which
  5. custommay be formed
  6. custompasses through both heating zones at an average residence time of 7.5 minutes
  7. custombeing 68° C. and that of the second one being 63° C.
  8. temperatureis then cooled to 25°-30° C

出典と根拠

ORDレコード
ord-a152ef1e533744db89e8ce5159cf60e5
出典データセット
uspto-grants-1994_11
特許番号
US05364954

反応ノート

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