化工社化工社 化学情報印刷レポート · 研究参考用
Ethene--prop-1-ene (1/1) → Ethylene/propylene 1-iodo-3-butene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethene--prop-1-ene (1/1) | HCID 62702 | — |
| 反応物 | Diethylaluminum iodide | HCID 74874 | — |
| 反応物 | 4-Iodobut-1-ene | HCID 543216 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | Ethylene/propylene 1-iodo-3-butene | HCID 86748291 | — |
反応手順
Into a 2 liter glass autoclave heated at the desidered temperature, toluene, 1-iodo-3-butene, V(acetylacetonate)3 and AlEt2I were introduced under nitrogen flow. A continuous constant ratio ethylene/propylene flow was then introduced.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05369186 |
| 出典データセット | uspto-grants-1994_11 |
| ORD ID | ord-173aa00af34e48d88f045ab52f42fcc0 |
| 出典メモ | uspto-grants-1994_11 |