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HRID 238359作成日:2026年10月26日

1-methyl-5-(2-phenylethenyl)-1H-pyrazole → 1-Methyl-5-(2-phenylethyl)-1H-pyrazole

https://huagongshe.com/reaction/238359

反応式

関与物質

役割名称HCID仕込み量
反応物1-methyl-5-(2-phenylethenyl)-1H-pyrazoleHCID 71401987—
触媒HCID 178418390HCID 178418390—
溶媒EthanolHCID 702—
生成物1-Methyl-5-(2-phenylethyl)-1H-pyrazoleHCID 86684862102.2%

反応手順

10% Palladium carbon (30 mg) was added to an ethanol (3.0 mL) solution of 1-methyl-5-(2-phenylethenyl)-1H-pyrazole (300 mg), and the obtained solution was then stirred under a hydrogen atmosphere at a room temperature for 14 hours. Thereafter, the reaction solution was filtrated with Celite, and the filtrate was then concentrated under a reduced pressure, so as to obtain the title compound (310 mg) in the form of a colorless oily substance.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US08642626B2
出典データセットuspto-grants-2014_02
ORD IDord-50ee3e6cf35c4f86b305a317eca7ecc6
出典メモuspto-grants-2014_02