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1-methyl-5-(2-phenylethenyl)-1H-pyrazole → 1-Methyl-5-(2-phenylethyl)-1H-pyrazole
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-methyl-5-(2-phenylethenyl)-1H-pyrazole | HCID 71401987 | — |
| 触媒 | HCID 178418390 | HCID 178418390 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | 1-Methyl-5-(2-phenylethyl)-1H-pyrazole | HCID 86684862 | 102.2% |
反応手順
10% Palladium carbon (30 mg) was added to an ethanol (3.0 mL) solution of 1-methyl-5-(2-phenylethenyl)-1H-pyrazole (300 mg), and the obtained solution was then stirred under a hydrogen atmosphere at a room temperature for 14 hours. Thereafter, the reaction solution was filtrated with Celite, and the filtrate was then concentrated under a reduced pressure, so as to obtain the title compound (310 mg) in the form of a colorless oily substance.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08642626B2 |
| 出典データセット | uspto-grants-2014_02 |
| ORD ID | ord-50ee3e6cf35c4f86b305a317eca7ecc6 |
| 出典メモ | uspto-grants-2014_02 |