Ethylenediamine → N~1~-(Pyridin-2-yl)ethane-1,2-diamine

HRID 238498

反応式

HRID 238498 の反応式
[CH2:1]([NH2:4])[CH2:2][NH2:3].F[C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][N:7]=1>>[N:7]1[CH:8]=[CH:9][CH:10]=[CH:11][C:6]=1[NH:3][CH2:2][CH2:1][NH2:4]

参加物

3

反応物 2

HCID 3301EthylenediamineHCID 97462-Fluoropyridine

生成物 1

HCID 410428N~1~-(Pyridin-2-yl)ethane-1,2-diamine

実験手順

Ethylenediamine (6 g, 0.1 mol) and 2-fluoropyridine (10 g, 0.1 mol) were heated neat at 120° C. overnight. The reaction was cooled and the residue was used in next step without further purification.

後処理

  1. temperatureThe reaction was cooled
  2. customthe residue was used in next step without further purification

出典と根拠

ORDレコード
ord-d13c71bd5af9458eb262afc0d4dc0739
出典データセット
uspto-grants-2014_02
特許番号
US08642624B2

関連ノート

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