2-Bromo-4-nitrophenol → 4-Amino-2-bromophenol

HRID 2386964ノート

反応式

HRID 2386964 の反応式
[Br:1][C:2]1[CH:7]=[C:6]([N+:8]([O-])=O)[CH:5]=[CH:4][C:3]=1[OH:11].[Cl-].[NH4+]>[Fe].CO>[NH2:8][C:6]1[CH:5]=[CH:4][C:3]([OH:11])=[C:2]([Br:1])[CH:7]=1

参加物

5

反応物 2

HCID 221092-Bromo-4-nitrophenol2 回HCID 25517Ammonium Chloride

生成物 1

HCID 144402654-Amino-2-bromophenol

試薬・触媒・溶媒 2

HCID 23925Iron触媒HCID 887Methanol溶媒

実験手順

The target compound was obtained by reducing 2-bromo-4-nitrophenol with iron in a mixed solution of methanol and ammonium chloride aqueous solution. 2-bromo-4-nitrophenol was manufactured by the method described in the literature (J. Org. Chem., Vol. 62, 1997, p. 4504).

後処理

  1. customThe target compound was obtained

出典と根拠

ORDレコード
ord-5a4a848ad6ad4a9bb141bd1e26fb4728
出典データセット
uspto-grants-2012_09
特許番号
US08268842B2

反応ノート

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