反応式
[CH:1]([N:3]([CH2:6][CH2:7][C:8]([O:10]CC)=O)[CH:4]=[O:5])=[CH2:2].[CH2:13]([NH2:16])[CH:14]=[CH2:15].C[O-].[Na+]>CO>[CH2:13]([NH:16][C:8](=[O:10])[CH2:7][CH2:6][N:3]([CH:1]=[CH2:2])[CH:4]=[O:5])[CH:14]=[CH2:15]参加物
5
反応条件
- 温度
- 90 °C
実験手順
A 100mL stainless steel high pressure reactor was charged with 17.1 grams (0.1 mol) of ethyl 3-(N-vinylformamido)propionate, 5.7 grams (0.1 mol) of allylamine and 0.15 gram of 25% sodium methoxide in methanol solution. The mixture was heated at 90° C. for 3 hours. Subsequent NMR analysis of the reaction mixture showed no conversion of the starting materials.
出典と根拠
- ORDレコード
- ord-e627c68d0c1743fc987ec32e90fb2b64
- 出典データセット
- uspto-grants-1998_03
- 特許番号
- US05728878
関連ノート
読み込み中…