化工社化工社 化学情報印刷レポート · 研究参考用
Dimethylamine → 3-bromo-N,N-dimethylbenzamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dimethylamine | HCID 674 | — |
| 反応物 | Benzoyl chloride, 3-bromo- | HCID 74377 | — |
| 反応物 | 4-(4-Bromobenzoyl)morpholine | HCID 532148 | — |
| 生成物 | 3-bromo-N,N-dimethylbenzamide | HCID 3335826 | 85% |
反応手順
Following the general method as outlined in Intermediate 174, starting from 3-bromobenzoyl chloride and dimethylamine, the title compound was obtained as a orange sticky solid in 85% yield.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08273769B2 |
| 出典データセット | uspto-grants-2012_09 |
| ORD ID | ord-45cbbc15817f4d2185f7d882de003a09 |
| 出典メモ | uspto-grants-2012_09 |