Oxalyl chloride → 2,6-Di(propan-2-yl)benzoyl chloride
反応式
[CH:1]([C:4]1[CH:12]=[CH:11][CH:10]=[C:9]([CH:13]([CH3:15])[CH3:14])[C:5]=1[C:6](O)=[O:7])([CH3:3])[CH3:2].C(Cl)(=O)C([Cl:19])=O>CN(C)C=O>[CH:1]([C:4]1[CH:12]=[CH:11][CH:10]=[C:9]([CH:13]([CH3:15])[CH3:14])[C:5]=1[C:6]([Cl:19])=[O:7])([CH3:3])[CH3:2]参加物
4
実験手順
A mixture of 2,6-diisopropylbenzoic acid (12.8 g, 0.062 mol), oxalyl chloride (25 mL), and dimethylformamide (2 drops) was stirred overnight at room temperature. The volatiles were removed on the rotary evaporator and the residue dried to yield an orange oil, 12.65 g, 90.9%.
後処理
- customThe volatiles were removed on the rotary evaporator
- customthe residue dried
- customto yield an orange oil, 12.65 g, 90.9%
出典と根拠
- ORDレコード
- ord-b0fb921268f647aa8967e6289c301e33
- 出典データセット
- uspto-grants-1998_09
- 特許番号
- US05807846
反応ノート
読み込み中…