Acetic Anhydride → HCID 136381103、化合物

HRID 2393653

反応式

HRID 2393653 の反応式
[NH2:1][C:2](=[N:20][N+:21]([O-:23])=[O:22])[NH:3][CH2:4][CH2:5][CH2:6][C@H:7]([C:9]([NH:11][CH2:12][C:13]1[CH:18]=[CH:17][C:16]([OH:19])=[CH:15][CH:14]=1)=[O:10])[NH2:8].[C:24](OC(=O)C)(=[O:26])[CH3:25]>C(O)(=O)C>[C:24]([NH:8][C@@H:7]([C:9]([NH:11][CH2:12][C:13]1[CH:14]=[CH:15][C:16]([OH:19])=[CH:17][CH:18]=1)=[O:10])[CH2:6][CH2:5][CH2:4][NH:3][C:2]([NH2:1])=[N:20][N+:21]([O-:23])=[O:22])(=[O:26])[CH3:25]

参加物

4

反応物 2

HCID 7918Acetic AnhydrideHCID 136381090(R)-N5-[amino(nitroimino)methyl]-N-[(4-hydroxyphenyl)methyl)-ornithinamide

生成物 1

HCID 136381103HCID 136381103、化合物

試薬・触媒・溶媒 1

HCID 176Acetic Acid溶媒

反応条件

温度
50 °C

実験手順

0.3 g (0.925 mMol) of (R)-N5 -[amino(nitroimino)methyl]-N-[(4-hydroxyphenyl)methyl]-ornithinamide were dissolved in 3 ml of glacial acetic acid and after the addition of 3 ml (0.032 Mol) of acetic anhydride the mixture was heated to a reaction temperature of 50° C. for 30 minutes. The product remaining after the volatile components had evaporated off was further processed without purification.

後処理

  1. customhad evaporated off
  2. customwas further processed without purification

出典と根拠

ORDレコード
ord-31ea9a0506fa40a8941c09e0e2b196c5
出典データセット
uspto-grants-1998_09
特許番号
US05807875

関連ノート

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