Glycine → Magnesium Glycinate

HRID 2397424

反応式

HRID 2397424 の反応式
C(=O)([O-])[O-].[Mg+2:5].[NH2:6][CH2:7][C:8]([OH:10])=[O:9].OCl>O>[NH2:6][CH2:7][C:8]([O-:10])=[O:9].[Mg+2:5].[NH2:6][CH2:7][C:8]([O-:10])=[O:9]

参加物

5

反応物 3

HCID 750GlycineHCID 11029Magnesium CarbonateHCID 24341Hypochlorous Acid

生成物 1

HCID 84645Magnesium Glycinate

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

Magnesium glycinate was prepared by reacting 3 g. of basic magnesium carbonate (26.1% Mg) with 5 g. of glycine in 40 g. of H2O, while agitating at 75° C. for one half hour. To the cooled slurry was added 100 g. of 33-1/3% zirconyl hydroxychloride solution (4.4% Zr) with agitation. After 15 minutes of stirring, the solution cleared and had a pH of 3.4. The product was oven-dried at 50° C. under a vacuum of 35 cm. of Hg, and found to contain 2.06% Mg, 36.9% Zr, and 13.1% glycine.

後処理

  1. additionTo the cooled slurry was added 100 g
  2. customThe product was oven-dried at 50° C. under a vacuum of 35 cm. of Hg

出典と根拠

ORDレコード
ord-47e92070f7184e29beaf50a9e45223c5
出典データセット
uspto-grants-1977_05
特許番号
US04021536

関連ノート

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