Acrylonitrile → 3-[(3,4-Dimethoxyphenethyl)Amino]Propanenitrile
反応式
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH2:11][CH2:12][NH2:13])[CH:6]=[CH:7][C:8]=1[O:9][CH3:10].[C:14](#[N:17])[CH:15]=[CH2:16]>CO>[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH2:11][CH2:12][NH:13][CH2:16][CH2:15][C:14]#[N:17])[CH:6]=[CH:7][C:8]=1[O:9][CH3:10]参加物
4
反応条件
- 温度
- 50 °C
実験手順
54.5 gm of 2-(3,4-dimethoxy-phenyl)-ethylamine were dissolved in 100 ml of methanol, a solution of 16.2 gm of acrylonitrile in 50 ml of methanol was added dropwise at 50° C, and the mixture was stirred for 1 hour at 50° C. After evaporation of the methanol, the raw reaction product thus obtained was used without further purification in the next step.
後処理
- customAfter evaporation of the methanol
- customthe raw reaction product
- customthus obtained
- customwas used without further purification in the next step
出典と根拠
- ORDレコード
- ord-5d876dcd569b41f6b08a33225a9a80dc
- 出典データセット
- uspto-grants-1977_05
- 特許番号
- US04021558
反応ノート
読み込み中…