1-Chlorooctadecane → Stearyl-[3-(p-Dimethylaminobenzamido)propyl]-Dimethylammonium Chloride

HRID 2399658

反応式

HRID 2399658 の反応式
[CH3:1][N:2]([CH3:18])[CH2:3][CH2:4][CH2:5][NH:6][C:7](=[O:17])[C:8]1[CH:13]=[CH:12][C:11]([N:14]([CH3:16])[CH3:15])=[CH:10][CH:9]=1.[CH2:19]([Cl:37])[CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH3:36]>>[Cl-:37].[CH2:19]([N+:2]([CH2:3][CH2:4][CH2:5][NH:6][C:7](=[O:17])[C:8]1[CH:13]=[CH:12][C:11]([N:14]([CH3:16])[CH3:15])=[CH:10][CH:9]=1)([CH3:18])[CH3:1])[CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH3:36]

参加物

3

反応物 2

HCID 188151-ChlorooctadecaneHCID 39788884-(dimethylamino)-N-[3-(dimethylamino)propyl]benzamide

生成物 1

HCID 67735953Stearyl-[3-(p-Dimethylaminobenzamido)propyl]-Dimethylammonium Chloride

実験手順

25.6 g of N-(3-dimethylaminopropyl)-p-dimethylaminobenzamide (0.103 mole) from Example 1 and 28.6 g of stearylchloride (0.099 mole) were melted together and kept at 130° C. for 3 hours. Product was crystallized from 250 ml of methylethylketone. Yield was 42 g (77% of theoretical yield).

後処理

  1. customProduct was crystallized from 250 ml of methylethylketone
  2. customYield was 42 g (77% of theoretical yield)

出典と根拠

ORDレコード
ord-c2948ff93b0a4e79828553c13ad7a958
出典データセット
uspto-grants-1995_09
特許番号
US05451394

関連ノート

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