2-Hex-1-enyl-1H-indole → HCID 14299246、化合物
反応式
[CH:1]([C:7]1[NH:8][C:9]2[C:14]([CH:15]=1)=[CH:13][CH:12]=[CH:11][CH:10]=2)=[CH:2][CH2:3][CH2:4][CH2:5][CH3:6]>C(O)C.[Pd]>[CH2:1]([C:7]1[NH:8][C:9]2[C:14]([CH:15]=1)=[CH:13][CH:12]=[CH:11][CH:10]=2)[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6]参加物
4
実験手順
2-Hex-1-enyl-1H-indole was dissolved in ethanol and 10% palladium on carbon was added to the solution. The reaction flask was sealed and exposed to hydrogen gas under pressure until the hydrogen gas consumption was stopped completely. The reaction mixture was filtered through Celite. The solvent was evaporated to afford the product.
後処理
- customThe reaction flask was sealed
- customexposed to hydrogen gas under pressure until the hydrogen gas consumption
- filtrationThe reaction mixture was filtered through Celite
- customThe solvent was evaporated
- customto afford the product
出典と根拠
- ORDレコード
- ord-5ef354922c5a4edf996e8a5ab0f148e7
- 出典データセット
- uspto-grants-2014_08
- 特許番号
- US08809382B2
反応ノート
読み込み中…