5-Chloro-2-hept-1-enyl-1H-indole → 5-chloro-2-heptyl-1H-indole
反応式
[Cl:1][C:2]1[CH:3]=[C:4]2[C:8](=[CH:9][CH:10]=1)[NH:7][C:6]([CH:11]=[CH:12][CH2:13][CH2:14][CH2:15][CH2:16][CH3:17])=[CH:5]2.[H][H]>C(O)C.[Pd]>[Cl:1][C:2]1[CH:3]=[C:4]2[C:8](=[CH:9][CH:10]=1)[NH:7][C:6]([CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH3:17])=[CH:5]2参加物
5
実験手順
5-Chloro-2-hept-1-enyl-1H-indole was dissolved in ethanol and 10% palladium on carbon was added to the solution. The reaction flask was sealed and exposed to hydrogen gas under pressure and was stirred for 5 hours. Then the reaction mixture was filtered through Celite. The solvent was evaporated to give 5-chloro-2-heptyl-1H-indole.
後処理
- customThe reaction flask was sealed
- filtrationThen the reaction mixture was filtered through Celite
- customThe solvent was evaporated
出典と根拠
- ORDレコード
- ord-e9b8d32c9bf04d95b837bc7e911d48a3
- 出典データセット
- uspto-grants-2014_08
- 特許番号
- US08809382B2
反応ノート
読み込み中…