Methyl iodide → 3,5-Dimethyl-2,4-Imidazolidinedione

反応式

[CH3:1][CH:2]1[NH:6][C:5](=[O:7])[NH:4][C:3]1=[O:8].[CH3:9]I>>[CH3:9][N:4]1[C:3](=[O:8])[CH:2]([CH3:1])[NH:6][C:5]1=[O:7]

参加物

反応物 2

HCID 6328Methyl iodide

HCID 692165-Methylhydantoin

生成物 1

HCID 101540613,5-Dimethyl-2,4-Imidazolidinedione

実験手順

Using 5-methylimidazolidine-2,4-dione (1.00 g) and methyl iodide (0.57 mL) and by the reaction and treatment in the same manner as in Preparation Example 214, the title compound (1.66 g, containing DMF) was obtained.

後処理

customby the reaction and treatment in the same manner
customas in Preparation Example 214

出典と根拠

ORDレコード: ord-6a391b4510b048bf8b2cb1df12641ef4
出典データセット: uspto-grants-2014_08
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US08816079B2

反応ノート

読み込み中…