Triethylamine → HCID 136347703、化合物
反応式
[C:1]([C:3]1[C:4](=[O:10])[NH:5][C:6](=[O:9])[NH:7][CH:8]=1)#[N:2].Cl.[NH2:12][OH:13].C(N(CC)CC)C>CO>[OH:13][N:12]=[C:1]([C:3]1[C:4](=[O:10])[NH:5][C:6](=[O:9])[NH:7][CH:8]=1)[NH2:2]参加物
5
実験手順
5-Cyano uracil (2.0 g, 14.6 mmol) was suspended in methanol (50 mL), then hydroxylamine hydrochloride (1.4 g, 20.0 mmol) and triethylamine (2.8 mL, 20.0 mmol) were added and the mixture was heated to reflux overnight. The mixture was cooled to room temperature, the solid was collected by filtration, washed with methanol and dried to give the title compound as a pale yellow solid (1.8 g).
後処理
- temperaturethe mixture was heated
- temperatureto reflux overnight
- filtrationthe solid was collected by filtration
- washwashed with methanol
- customdried
出典と根拠
- ORDレコード
- ord-847b5d1e0bfe4579a03ca873d9a9f2b9
- 出典データセット
- uspto-grants-2004_11
- 特許番号
- US06821972B2
反応ノート
読み込み中…