反応式
[CH3:1][O:2][C:3]([P:5](=[O:12])([O:9][CH2:10][CH3:11])[O:6]CC)=[O:4].[I-].[Na+:14]>O1CCCC1>[CH3:1][O:2][C:3]([P:5](=[O:6])([OH:12])[OH:9])=[O:4].[CH2:10]([Na:14])[CH3:11]参加物
4
実験手順
A solution of 5.9 parts of diethyl methoxycarbonylphosphonate and 4.5 parts of sodium iodide was stirred at room temperature in 50 parts of tetrahydrofuran for 60 hours. The resulting mixture was filtered to give 3.5 parts of the desired ethyl sodium methoxycarbonylphosphonate, m.p. 123° d.
後処理
- filtrationThe resulting mixture was filtered
出典と根拠
- ORDレコード
- ord-04a7421230c04887bbc12f7c2e1c8d77
- 出典データセット
- uspto-grants-1978_08
- 特許番号
- US04108626
関連ノート
読み込み中…