Sodium Hydroxide → HCID 178452788、化合物

HRID 24809

反応式

HRID 24809 の反応式
C([N:4]1[C:12]2[C:7](=[CH:8][C:9]([N+:13]([O-:15])=[O:14])=[CH:10][CH:11]=2)[C:6](=[C:16](OC)[C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)[C:5]1=[O:25])(=O)C.[C:26]([O:30][C:31]([NH:33][C:34]1[CH:40]=[CH:39][C:37]([NH2:38])=[CH:36][CH:35]=1)=[O:32])([CH3:29])([CH3:28])[CH3:27].[OH-].[Na+]>CN(C=O)C.CO>[C:26]([O:30][C:31]([NH:33][C:34]1[CH:35]=[CH:36][C:37]([NH:38]/[C:16](=[C:6]2\[C:5](=[O:25])[NH:4][C:12]3[C:7]\2=[CH:8][C:9]([N+:13]([O-:15])=[O:14])=[CH:10][CH:11]=3)/[C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)=[CH:39][CH:40]=1)=[O:32])([CH3:29])([CH3:27])[CH3:28]

参加物

6

反応物 3

HCID 14798Sodium HydroxideHCID 688611tert-Butyl (4-aminophenyl)carbamateHCID 541401551-Acetyl-3-(1-methoxy-1-phenyl-methylidene)-5-nitro-2-indolinone

生成物 1

HCID 178452788HCID 178452788、化合物

試薬・触媒・溶媒 2

HCID 887Methanol溶媒HCID 6228Dimethylformamide溶媒

実験手順

Prepared analogously to Example 82 from 1-acetyl-3-(1-methoxy-1-phenyl-methylidene)-5-nitro-2-indolinone and 4-tert.butoxycarbonylamino-aniline in DMF and subsequent treatment with sodium hydroxide solution in methanol.

出典と根拠

ORDレコード
ord-c00a7cb5bdf94b7983b3c440073516b0
出典データセット
uspto-grants-2005_02
特許番号
US06855710B2

関連ノート

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