反応式
[CH3:1][C:2]([CH3:12])=[CH:3][C:4]1[CH:5]=[C:6]([CH:9]=[CH:10][CH:11]=1)[C:7]#[N:8]>CO.[Pd]>[CH2:3]([C:4]1[CH:5]=[C:6]([CH:9]=[CH:10][CH:11]=1)[C:7]#[N:8])[CH:2]([CH3:12])[CH3:1]参加物
4
反応条件
- 温度
- 25 °C
実験手順
To a solution of 3-(2-methyl-1-propenyl)benzonitrile (5.80 g) in methanol (50 ml) was added 10% palladium on activated carbon (1 g), and the mixture was stirred under hydrogen atmosphere (3 atm) at 25° C. for 1 hour. The catalyst was filtered off and the filtrate was evaporated to give 3-isobutylbenzonitrile (5.52 g) as a pale yellow oil.
後処理
- filtrationThe catalyst was filtered off
- customthe filtrate was evaporated
出典と根拠
- ORDレコード
- ord-d6481656cfa043db90ae1011ec48aef2
- 出典データセット
- uspto-grants-1993_05
- 特許番号
- US05212320
関連ノート
読み込み中…