Diethyl Carbonate → Carbonic acid, bis[2-(dimethylamino)ethyl] ester
反応式
CN(C[CH2:5][O:6][CH2:7][CH2:8][N:9]([CH3:11])[CH3:10])C.[CH3:12][N:13]([CH2:15][CH2:16][OH:17])[CH3:14].C(=O)(OCC)[O:19]CC>>[CH3:12][N:13]([CH2:15][CH2:16][O:17][C:5](=[O:19])[O:6][CH2:7][CH2:8][N:9]([CH3:10])[CH3:11])[CH3:14]参加物
4
実験手順
A process for preparing bis[2-(N,N-dimethylamino)ethyl]ether which comprises (i) contacting 2-(N,N-dimethylamino)ethanol with diethyl carbonate under conditions effective to produce bis[2-(N,N-dimethylamino)ethyl]carbonate, and (ii) contacting bis[2-(N,N-dimethylamino)ethyl]-carbonate with a magnesium:aluminum mixed metal oxide catalyst under conditions effective to produce bis[2-(N,N-dimethylamino)ethyl]ether.
出典と根拠
- ORDレコード
- ord-696a3e0ca432431dbb0c5737154e8fbe
- 出典データセット
- uspto-grants-1993_05
- 特許番号
- US05214142
反応ノート
読み込み中…