Cyanamide → HCID 86619051、化合物
反応式
[F:1][C:2]([F:8])([F:7])[CH2:3][CH2:4][CH:5]=O.N1CCCC1.O.C1(C)C=CC([S:21](O)(=O)=O)=CC=1.[S].[N:27]#[C:28][NH2:29]>>[F:1][C:2]([F:8])([F:7])[CH2:3][C:4]1[S:21][C:28]([NH2:29])=[N:27][CH:5]=1参加物
6
実験手順
A mixture of 4,4,4-trifluorobutyraldehyde (Matrix), pyrrolidine, p-toluenesulfonic acid monohydrate, sulfur and cyanamide were processed using the method described in Example 136A to obtain the title compound. MS (ESI+) m/z 183 (M+H)+.
出典と根拠
- ORDレコード
- ord-d761a2f406114e86992dfc1ff0d839d1
- 出典データセット
- uspto-grants-2011_01
- 特許番号
- US07875639B2
反応ノート
読み込み中…