Isopropylamine → HCID 178457516、化合物
反応式
C(N[CH:4]=[N:5][C:6]1[CH:11]=[CH:10][C:9]([C:12]2[N:16]=[CH:15][NH:14][N:13]=2)=[CH:8][CH:7]=1)#N.[CH:17]([NH2:20])([CH3:19])[CH3:18]>O>[CH:17]([NH:20][CH:4]=[N:5][C:6]1[CH:11]=[CH:10][C:9]([C:12]2[N:16]=[CH:15][NH:14][N:13]=2)=[CH:8][CH:7]=1)([CH3:19])[CH3:18]参加物
4
実験手順
A solution of N-Cyano-N'-[4-(1,2,4-triazol-3-yl)-phenyl]-formamidine (3 g) and isopropylamine (8.5 g) in water (1.5 ml) was stirred for twenty minutes. The crystallized solid was filtered off and purified via its maleate salt in ethanol.
後処理
- filtrationThe crystallized solid was filtered off
- custompurified via its maleate salt in ethanol
出典と根拠
- ORDレコード
- ord-fe2fe274ad4e4573b6aea4ebe09a8706
- 出典データセット
- uspto-grants-1987_10
- 特許番号
- US04699915
反応ノート
読み込み中…