Triethylenetetramine → Ethylene carbonate triethylene tetraamine

HRID 256296

反応式

HRID 256296 の反応式
[NH2:1][CH2:2][CH2:3][NH:4][CH2:5][CH2:6][NH:7][CH2:8][CH2:9][NH2:10].[C:11]1(=[O:16])[O:15][CH2:14][CH2:13][O:12]1>C1(C)C=CC=CC=1>[C:11]1(=[O:16])[O:15][CH2:14][CH2:13][O:12]1.[NH2:1][CH2:2][CH2:3][NH:4][CH2:5][CH2:6][NH:7][CH2:8][CH2:9][NH2:10]

参加物

4

反応物 2

HCID 5565TriethylenetetramineHCID 7303Ethylene carbonate

生成物 1

HCID 86740738Ethylene carbonate triethylene tetraamine

試薬・触媒・溶媒 1

HCID 1140Toluene溶媒

実験手順

Add 2 g of triethylene tetraamine (with an AV of approximately 1180 mg KOG/g) to 20 ml of toluene in a 250 ml flask fitted with a stirrer, condensor and nitrogen inlet. Add 27.6 g ethylene carbonate to the mixture. Reflux the system for 2.5 hours under N2. Strip the system to yield an ethylene carbonate-triethylene tetraamine adduct having an AV of approximately 104 mg KOH/g.

後処理

  1. customfitted with a stirrer
  2. temperatureReflux the system for 2.5 hours under N2

出典と根拠

ORDレコード
ord-5b44c79bf23141248387f678a3e30198
出典データセット
uspto-grants-1987_10
特許番号
US04702851

関連ノート

読み込み中…