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2,3,4,5-Tetramethylpyridine → Phthalocyanine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2,3,4,5-Tetramethylpyridine | HCID 87644 | — |
| 反応物 | CID 136122626 | HCID 136122626 | — |
| 生成物 | Phthalocyanine | HCID 86280045 | — |
反応手順
For this preparation, dilithiated lithium phthalocyanine is contacted with (2H)-2,2,6,6-tetramethylpiperidine. The latter was prepared by H-D isotopic exchange between commercially available tetramethylpyridine (TMP) and 2H2O at ambient temperature, followed by a separation of the organic phase and the aqueous phase by ether addition.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05258313 |
| 出典データセット | uspto-grants-1993_11 |
| ORD ID | ord-0172df0db5aa4bbc92d75b5aa16205b4 |
| 出典メモ | uspto-grants-1993_11 |