EP-302 → Dimethyl Phthalate
反応式
CC(C1C=CC(O)=CC=1)(C1C=CC([OH:10])=CC=1)C.[CH2:18]1[O:20][CH:19]1[CH2:21]Cl.[C:23]1(=O)OCCC[CH2:31][O:30][C:28](=[O:29])[C:27]2C=C[C:24]1=[CH:25][CH:26]=2>[I-].C1(C(C2C=CC=CC=2)(C2C=CC=CC=2)C[PH3+])C=CC=CC=1>[CH3:18][O:20][C:19](=[O:10])[C:21]1[C:27](=[CH:26][CH:25]=[CH:24][CH:23]=1)[C:28]([O:30][CH3:31])=[O:29]参加物
4
実験手順
Epikote 1004 (180 g), a homopolymer of butylene terephthalate (120 g) and triphenylethyl phosphonium iodide (0.3 g) were melt blended in an extruder as described in Composition 1. A sample of the solidified resulting mixture (30 g) and dimethylphthalate (10 g) were heated in a beaker to 260° C. and poured into butyl diglycol acetate (120 g) at 125° C. The mixture was dispersed using a Silverson high speed stirrer for 3 minutes during which time the temperature rose to 140° C. The mixture was cooled using an ice bath, reaching 49° C. within one minute. The resulting dispersion had a non-volatile content of 18.7% and a particle size range of 0.5 to 10μ.