Methyl iodide → 3-(3-(3-Methyl-2-butenyloxy)-1,2,5-thiadiazol-4-yl)-1-methylpyridinium iodide
反応式
[CH3:1][I:2].[CH3:3][C:4]([CH3:19])=[CH:5][CH2:6][O:7][C:8]1[C:9]([C:13]2[CH:14]=[N:15][CH:16]=[CH:17][CH:18]=2)=[N:10][S:11][N:12]=1>CC(C)=O>[I-:2].[CH3:3][C:4]([CH3:19])=[CH:5][CH2:6][O:7][C:8]1[C:9]([C:13]2[CH:14]=[N+:15]([CH3:1])[CH:16]=[CH:17][CH:18]=2)=[N:10][S:11][N:12]=1参加物
4
実験手順
A mixture of methyl iodide (1 ml, 15 mmol) and 3-(4-(3-methyl-2-butenyloxy)-1, 2,5-thiadiazol-3-yl)pyridine (3 mmol) in acetone (3 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 0.92 g (79%).
後処理
- customThe title compound precipitated from the solution
- filtrationwas collected by filtration
- customto yield 0.92 g (79%)
出典と根拠
- ORDレコード
- ord-46175e62c42b485da758bb668c60022d
- 出典データセット
- uspto-grants-1993_11
- 特許番号
- US05260311
反応ノート
読み込み中…