4-Ethylpyridine → 1-(2,6-Dichlorophenyl)-3-(4-pyridyl)butane

HRID 257467

反応式

HRID 257467 の反応式
[CH2:1]([C:3]1[CH:8]=[CH:7][N:6]=[CH:5][CH:4]=1)[CH3:2].[Cl:9][C:10]1[CH:18]=[CH:17][CH:16]=[C:15]([Cl:19])[C:11]=1[CH2:12][CH2:13]Br>>[Cl:9][C:10]1[CH:18]=[CH:17][CH:16]=[C:15]([Cl:19])[C:11]=1[CH2:12][CH2:13][CH:1]([C:3]1[CH:8]=[CH:7][N:6]=[CH:5][CH:4]=1)[CH3:2]

参加物

3

反応物 2

HCID 108224-EthylpyridineHCID 134801952-(2-Bromoethyl)-1,3-dichlorobenzene

生成物 1

HCID 197833131-(2,6-Dichlorophenyl)-3-(4-pyridyl)butane収率 55.3%

実験手順

1.0 g (9.35 mmol) of 4-ethylpyridine and 2.37 g (9.35 mmol) of 2,6-dichlorophenethyl bromide were reacted in the same manner as in Example 1. The reaction product was purified to obtain 1.45 g of the desired compound (yield: 55.3%). The resulting compound was identified as 1-(2,6-dichlorophenyl)-3-(4-pyridyl)-butane (hereinafter referred to as compound 11) by the following analytical results.

後処理

  1. customThe reaction product was purified

出典と根拠

ORDレコード
ord-ee4c7f6b2d9949818626607b3a34d2d8
出典データセット
uspto-grants-1993_11
特許番号
US05262420

関連ノート

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