Phenethyl bromide → HCID 19783335、化合物

反応式

[CH2:1]([C:3]1[CH:4]=[N:5][CH:6]=[CH:7][C:8]=1[CH2:9][CH3:10])[CH3:2].[CH2:11](Br)[CH2:12][C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1>>[C:13]1([CH2:12][CH2:11][CH:9]([C:8]2[CH:7]=[CH:6][N:5]=[CH:4][C:3]=2[CH2:1][CH3:2])[CH3:10])[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1

参加物

反応物 2

HCID 7666Phenethyl bromide

HCID 691513,4-Diethylpyridine

生成物 1

HCID 19783335HCID 19783335、化合物収率 57.2%

実験手順

1.26 g (9.35 mmol) of 3,4-diethylpyridine and 1.73 g (9.35 mmol) of phenethyl bromide were reacted in the same manner as in Example 1. The reaction product was purified to obtain 1.28 g of the desired compound (yield: 57.2).

後処理

customThe reaction product was purified

出典と根拠

ORDレコード: ord-3e184518fda64d6594a532445f7fa8d7
出典データセット: uspto-grants-1993_11
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US05262420

反応ノート

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