反応式
C(SCC1[C:15]2[C:10](=[CH:11][CH:12]=[C:13](C3C=CC=CC=3)[CH:14]=2)[NH:9]C(C)(C)C=1)C=C.Br[CH2:25][C:26]1[C:35]2[C:30](=[CH:31][CH:32]=[C:33]([C:36]3[CH:41]=[CH:40][CH:39]=[CH:38][C:37]=3[O:42][CH3:43])[CH:34]=2)[NH:29][C:28]([CH3:45])([CH3:44])[CH:27]=1.C(=O)([O-])[O-].[K+].[K+].C(S)C=C>>[CH3:43][O:42][C:37]1[CH:38]=[CH:39][CH:40]=[CH:41][C:36]=1[C:33]1[CH:34]=[C:35]2[C:30](=[CH:31][CH:32]=1)[NH:29][C:28]([CH3:45])([CH3:44])[CH:27]=[C:26]2[CH2:25][NH:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1参加物
5
反応物 4
生成物 1
実験手順
4-Allylsulfanylmethyl-2,2-dimethyl-6-phenyl-1,2-dihydroquinoline 40 mg of 4-bromomethyl-6-(2-methoxyphenyl)-2,2-dimethyl-1,2-dihydroquinoline, 46 mg of potassium carbonate, and 44 μL of allyl mercaptan reacted to give 5 mg of the title compound as an oil.
出典と根拠
- ORDレコード
- ord-152309d9e4b24a4dbec8c8e16c163aa9
- 出典データセット
- uspto-grants-2005_02
- 特許番号
- US06858627B2
関連ノート
読み込み中…