4-Bromobutyryl chloride → 5-(4-Diethylamino-butyryl)-5,10-dihydro-11H-dibenzo(b,e)(1,4)-diazepine-11-one

HRID 257745

反応式

Br[CH2:2][CH2:3][CH2:4][C:5]([N:7]1[C:13]2[CH:14]=[CH:15][CH:16]=[CH:17][C:12]=2[C:11](=[O:18])[NH:10][C:9]2[CH:19]=[CH:20][CH:21]=[CH:22][C:8]1=2)=[O:6].C1C2C(=O)N[C:30]3C=CC=C[C:29]=3[NH:28][C:27]=2[CH:26]=CC=1.BrCCCC(Cl)=O>C1(C)C=CC=CC=1>[CH2:27]([N:28]([CH2:29][CH3:30])[CH2:2][CH2:3][CH2:4][C:5]([N:7]1[C:13]2[CH:14]=[CH:15][CH:16]=[CH:17][C:12]=2[C:11](=[O:18])[NH:10][C:9]2[CH:19]=[CH:20][CH:21]=[CH:22][C:8]1=2)=[O:6])[CH3:26]

参加物

実験手順

The 5-(4-bromobutyryl)-5,10-dihydro-11H-dibenzo(b,e)(1,4)-diazepine-11-one, starting material, was synthesized similarly to the starting material described in Example 1, from 5,10-dihydro-11H-dibenzo(b,e)(1,4)-diazepine-11-one and 4-bromobutyryl chloride. The yield is 74.3% of the theoretical yield and the melting point is 159°-161° C. (toluene).

後処理

customwas synthesized similarly to the starting material
customThe yield is 74.3% of the theoretical yield

出典と根拠

ORDレコード: ord-d7b8681b86894f4c8a6680f86fef89c1
出典データセット: uspto-grants-1993_11
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US05264432

反応式

参加物

反応物 3

生成物 1

試薬・触媒・溶媒 1

実験手順

後処理

出典と根拠

関連ノート